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vi CONTENTS 2.4.2 Sabatieranalysis ...................... 38 2.4.3 Scalingrelations ...................... 39 3 Experimental methods 43 3.1 Preparation of mixed oxide coatings using spin-coating . . . . . . 43 3.2 Electrochemicalmeasurements................... 44 3.2.1 Cyclicvoltammetry..................... 44 3.2.2 Galvanostatic polarization curve measurements . . . . . . 44 3.3 Combined determination of gas-phase and liquid-phase composi- tions during hypochlorite decomposition using mass spectrometry andionchromatography ...................... 46 4 Results and discussion 47 4.1 Co-dopedRu-Tidioxideelectrocatalysts . . . . . . . . . . . . . . 47 4.2 SelectivitybetweenCl2andO2 ................... 48 4.2.1 The uncatalyzed and catalyzed decomposition of hypochlo- ritespecies ......................... 48 4.2.2 Theoretical studies of the connection between oxide com- position and ClER and OER activity and selectivity . . . . 53 4.3 Semiclassicalmodelingofrutileoxides . . . . . . . . . . . . . . 66 4.4 XPSmodeledusingDFT ...................... 69 4.4.1 TheactivesiteforHERonMoS2 ............. 70 4.4.2 StructuralchangesinRuO2 duringHER . . . . . . . . . . 73 5 Conclusions and recommendations 79 5.1 Conclusions............................. 79 5.2 Recommendationsforfuturework ................. 80 6 Bibliography 85 7 Acknowledgments 99PDF Image | Studies of Electrode Processes in Industrial Electrosynthesis
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