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Studies of Electrode Processes in Industrial Electrosynthesis

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Studies of Electrode Processes in Industrial Electrosynthesis ( studies-electrode-processes-industrial-electrosynthesis )

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4.4. XPSMODELEDUSINGDFT 75 Figure 4.19: Ru 3d (left) XPS spectra of RuO2/Ni cathodes and metallic Ru and O 1s (right) XPS spectra of RuO2/Ni cathodes. (a) is a reference RuO2/Ni sample, that has not been exposed to the electrolyte, (b)-(g) are measurements on electrodes used for hydrogen evolution for either 0.5 h, 3 h, 6 h, 12 h, 18 h or 24 h, respectively and (h) in the left figure is a spectrum from metallic Ru. Figures reprinted with permission from Näslund et al. [51]. Copyright 2014 American Chemical Society.

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