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ll iScience OPEN ACCESS Article Figure 8. IR and Raman analysis of cathodes at various charge/discharge states (A) IR spectra of carbon black. (B) Raman spectrum of graphene. energies of the Cl 2p of the carbon cathode when the battery is fully charged; therefore, no chemical change of chlorine can be evidenced, which remains as Cl ions, indicating that the s Cl ions deintercalate from the carbon cathode and are captured by metal anode during the battery discharge process. As shown in Figure 10B, two peaks of 1,021.8 and 1,044.8 eV are observed in the Zn 2p core level spectrum, indicating that Zn atoms are in an intermediate state of metal Zn2+ and zinc (Wu et al., 2017b; Naveed et al., 2019). For electrolyte, Figure 10D shows the existence of Cl 2p, C1s, N1s, and O1s without Zn signals, indicating that Figure9. XPSspectraofcarbonblackcathodesurfaceandelementalmappingimageswhenthebatterywasfully charged (A) Carbon black surface region. (B) Cl 2p. (C) C1s. (D) O1s. 10 iScience 24, 101976, January 22, 2021PDF Image | aqueous chlorine ion battery
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