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Figure 2. Zn/ClO2 full cell and test results. (a) Photograph of the proof of concept Zn/ClO2 full cell used in this study is shown in the left and center image, while an exploded view showing individual components appears at the right. In the center image, the dashed line separates the fluid levels for the aqueous electrolyte and organic solvent. (b) The full cell voltage vs capacity for the Zn/ClO2 cell in (a), cycled under constant current charge at 5mA/cm2 with a capacity cut off at 10mAh followed by a constant current discharge at 5mA/cm2 to a lower voltage of 0.8V. The testing temperature was 0.5°C ± 0.5°C. The positive electrolyte consists of a 1.5 mL volume of 1.95 mol/L NaClO2 solution, on top of which floats 6 mL of a hydrocarbon solvent in which ClO2 is soluble. The negative electrolyte consists of a 3 mL volume having 0.96 mol/L ZnCl2 and 0.98 mol/L NaCl. A silver/silver chloride (Ag/AgCl) wire pseudo reference electrode was placed in the negative electrolyte of the cell. A piece of sodiated Nafion 117 (Na-N117) separated the positive electrolyte and the negative electrolyte. (c) The cathode vs reference electrode voltage for the cell in Fig. 2b. No ohmic corrections have been performed; the ohmic resistance between the cathode and the reference electrode is about 18 ohm under the testing condition. 7PDF Image | Reversible Chlorite Chlorine Dioxide Anion Redox Storage
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