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4.2. SELECTIVITY BETWEEN CL2 AND O2 51 0.12 0.1 0.08 0.06 0.04 0.02 0 4 3 2 1 0 456789 a) pH b) 456789 pH Figure 4.4: a) The maximum rates of uncatalyzed oxygen (estimated based on flow of oxygen at the MS detector) and b) chlorate formation (based on the initial rate). Both processes have similar pH dependence, signaling a possible connection between the two reaction pathways. Reprinted with permission from Sandin et al. [14]. Copyright 2015 American Chemical Society. 1 0.5 0 0 20 40 60 80 time / min 3rd order 2nd order Data average Figure 4.5: The experimental data for accumulated oxygen (per electrolyte vol- ume) together with fitted second- and third-order rate expressions indicating that a third-order rate expression is a better description of the data. Reprinted with permission from Sandin et al. [14]. Copyright 2015 American Chemical Society. CO / mM 2 R - / mM ·min -1 FO max / mM ·min -1 2 i,ClO 3PDF Image | Studies of Electrode Processes in Industrial Electrosynthesis
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