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Investigation, and Writing – Review and Editing; H.P.: Methodology and Investigation T.M.A.: Writing – Review and Editing, Resources and Supervision Y.P.: Writing – Review and Editing, Supervision and Funding Acquisition Notes The authors declare no competing financial interest. ACKNOWLEDGMENT This work was funded by the U.S. Department of Energy, Office of Electricity, Energy Storage program under Dr. Imre Gyuk, Program Director. Sandia National Laboratories is a multimission laboratory managed and operated by National Technology & Engineering Solutions of Sandia, LLC, a wholly owned subsidiary of Honeywell International, Inc., for the U.S. DOE’s National Nuclear Security Administration under contract DE-NA-0003525. The views expressed in the article do not necessarily represent the views of the U.S. DOE or the United States Government. SAND2022-13143 O We thank Dr. Jessica Kustas and David Schafer for calibrating the UGA system. We also thank Mike Perry for his help in developing the parameters for the scale up calculations. We thank Brittney Flores for her help making the graphics used in the TOC and Figure 4. We thank Dr. Leo Small for critical review of the manuscript. We thank Alex Bates for his help in troubleshooting aspects of the UGA gas capillary connection. REFERENCES: 1. Wittman, R. M.; Perry, M. L.; Lambert, T. N.; Chalamala, B. R.; Preger, Y., Perspective—On the Need for Reliability and Safety Studies of Grid-Scale Aqueous Batteries. J. Electrochem. Soc. 2020, 167 (9), 90545. 2. Patterson, M. Battery Storage Container Explodes, Rocking Rio Dell RV Park. https://krcrtv.com/north-coast-news/eureka-local-news/battery-storage-container-explodes- rocking-rio-dell-rv-park (accessed 08/30/2022). 3. Rychcik, M.; Skyllas-Kazacos, M., Characteristics of a new all-vanadium redox flow battery. J. Power Sources 1988, 22, 59-67. 4. Airgas Chlorine Safety Data Sheet. https://www.airgas.com/msds/001015.pdf. 13PDF Image | Chlorine Gas Generation in Mixed-Acid Vanadium Redox
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